UNIT OPERATIONS: Separation / Purification

Enrichment of High Fructose Syrup

- an example for a new chromatography application

fructose

High Fructose (Corn) Syrup - HFS or HFCS - is a nutritive sweetener with high commercial potential. It is a product in which a large percentage of the glucose - derived from starch hydrolysis - has been converted into its sweeter-tasting isomer fructose, by the use of enzymes. The crystal clear syrup has a sweetness and calories approximately equal to that of a sugar solution. It performs many of the same functions as sugar, chiefly the "clean" sweetening of beverages,  ketchup, dairy products, baked goods, and so on. HFS is usually sold at a price considerably below sugar, hence its popularity.

     Why enrichment?

Fructose syrups obtained by isomerisation of glucose have less sweetening power than sucrose. For the use as a substitute of sucrose it is necessary to improve the sweetness of the syrup.

Therefore the fructose content of around 42% of dry matter substance (dms)  has to be enriched to a fructose content of 55% dms, to comply with industrial product standards.

     How?

The enrichment of fructose by low cost chromatographic methods in a so-called moving bed process is effectively state-of-the-art. The main object of such a process is to fractionate fructose-glucose syrup into a 90% fructose syrup product (HFS90).

To produce enriched fructose syrup with 55% fructose content (HFS55), original fructose-glucose syrup is blended with HFS90. As HFS90 only has a dms of 35%, the blended mixture is concentrated by evaporation to ensure durability of the product.

     block diagram - click to view PDF file  
PDF files require Acrobat Reader

      The Vogelbusch HFS process

Vogelbusch's HFS process is based on the use of starch as a raw material, obtained from sources such as corn, wheat, cassava a.s.o.

The block diagram (PDF) diagram gives a principle overview of the process steps in HFS production and the production of glucose monohydrate and anhydrous glucose with special focus on the latest development, a process and special equipment for the production of HFS90 for blending to syrups with lower fructose contents.

Concentration profile (PDF) - Continuous, inline measurement of refraction and polarisation of the circulating liquid fluid enables the display of the actual concentration profile in the adsorbent bed as a diagram on the computer screen, thus permitting fine-tuning of the process to achieve optimum operating performance of the system.

 

Apart from HFS enrichment, the system can be used for various applications, for instance in molasses saccharfication.

 

INTRODUCTION

EXAMPLE: High Fructose Syrup (HFS) Enrichment

 

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Last modified: 19.12.03 by HaK

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